TURK STANDARDI
Transkript
TURK STANDARDI
TURK STANDARDI TS EN 590 $ubat 20'14 TS EN 590+41:2010 yerine tcs 75.160.20 Otomotiv yakrtlan - Dizel (motorin) - Gerekler ve deney y6ntemleri Automotive fuels - Diesel - Requirements and test methods Carburants pour automobiles - Carburants pour moteur - Exigences et methodes (gazole) diesel d'essai Kraft stoffe fU r Kraftf ah rzeu ge - Dieselkraft stoff Anforderungen und Prtlfuerfahren TURK STANDARDLARI ENSTiTUSU Necatibey Caddesi No.112 Bakanlrklar/ANKARA TSE DEN izrN ALINI{ADAN SIANDARD|N &R BOLU|\iUIIAMAI',|| iL I,BAS EDiLEMEZ, QOGALTILAMAZ ICS 75.160.20 TS EN 590 : 2014-02 TURK STANDARDI Bu standard, CEN/TC 19 "Gaseous and liquid fuels, lubricants and related products of petroleum, synthetic and biological origin - Biyolojik ve sentetik esaslr gaz ve srvr yakrlar, yaglama yaglal ve ilgili Urunlei' Teknik Komitesi tarafrndan hazrrlanmrg, cEN tarafrndan 26.01.2013 tarihinde onaylanmrg ve Turk Standardlan Enstitosu Teknik Kurulu'nu n 13.02.2014 tarihli toplanttstnda T0rk Standardt olarak kabul edilerek yayrmrna karar verilmigtir. Bu standardda kullanllan bazt kelimeler ve/veya ifadeler patent haklanna konu olabitir. Bdyle patent hakktntn belirlenmesi durumunda TSE sorumlu tutulamaz. bir Bu standard yayrnlandrgrnda TS EN 590+41:2010 standardrntn yerini alrr. cEN uyeleri srrasryra,Armanya, Avusturya, Bergika, Birregik KraIrk, Burgaristan, eek cumhuriyeti, Danimarka, Estonya, Finrandiya, Fransa, Hrrvatlstan, HoIanda, lrranda,lspanya, lsve!, lsvigre, ltarya, lzlanda, Krbns, Letonya, Litvanya, Li,ksemburg, Macaristan, Makedonya, Marta, Norveg, poronya, Portekiz, Romanya, Slovakya, slovenya, Turkiye ve yunanistan'rn milli standard kuruluglandrr. TS EN 590 2014 slandardr. Brussels) rzniyle basrlmtslrr. iiye rllkeleane EN 590:2013 standardr ile bircbir aynr otup, Avruf,a Standardizasyon Xomitesitinl renue Marnix i7. B-.tOOO TS EN 590 : 2014-02 EUROPEAN STANDARD EN 590 NORME EUROPEENNE EUROPAISCHE NORM September 20'13 lcs 75.160.20 Supersedes EN 590:2009+4'1 :201 O English Version Automotive fuels - Diesel - Requirements and test methods Caduranls pour automobiles - Carburants pour moteur Kraftstoffe fur Kraftfahzeuge - Dieselkraftsloff Anforderungen und Prufverfahren diesel (gazole) - Exiqences et methodes d'essai Thas European Standard was approved by CEN on 26 July 2013. CEN members are bound to comply with the CEN/CENELEC lntemal Regulations \4rhich slipulale the conditions for giving this European Slandard the status of a national standard wilhout any alteration. Up-to{ile lists and bibliographacal references coniemiig such nalional standards may be obtained on applic€tion lo ihe CEN-CENELEC Management Centre or ttany CEN member. This European Standard exists in three official versions (English, French, German). A version in any other language made by translation under the respoisibility of a CEN member anto ils own language and notified to the CEN-CENELei vanagem-enttentre hai lhe same stalus as the official versions. CEN members are the national standards bodies ofAustria, Belgium, Bulgaria, Croatia, Cyprus, Czech Repubtic, Denmark, Estonaa, Finland, Former Yugoslav Republic of Macedonia, France, Germany, Greece, Hungary, tdland, lreland, ldly, Latvia, Lithuania, Luxembourg, Malla, Netherlands Norway, Poland, Portugal, Romania, Slovakia, Siov;nia, Spain, Sweden, Switzerland, Tu*ey and United Kingdom. E EUROPEAN COMMITTEE FOR STANDARDIZATION COMITE EUROPEEN DE NORN,IALISATION EUROPAIScHES KoMITEE FUR NoRMUNc Management Csntro: AvEnue Marnlx 17, B-IOOO Brussols O 2013 CEN All righls of exploitalion in any form and by any means reserved ',lorldwide Rel No. for CEN nationat Members. ruRK STAN0ARDLARININ TEI'F hAKKI TSE Y! ArTTiR. SIANDARDtN BU NUSHASTNTN KiILLAN|M izNr TSE TARAFTNDAN TURKiYE VAGON SANAYiiA.S.'A VER,LiliSTiF. BAStLt A IARiHi: 15.07.20i5 TSE'DEN iZ'N ALIN[,1ADAN STANDARDIN BiR BOLUiTUiIAMAMt TLTTBAS EDiLEMEZ, COGALTTLAMAZ. EN 590:2013 E TS EN 590 : 2014-02 EN 590:2013 (E) Contents Page Foreword ...........3 2 Normative references 3 Sampling 4 Pump marking 5 5.'t 5.2 5.2.1 5.2.2 5.3 5.4 5.5 5.6 5.7 Other (bio, components............... Generally applicable requirements and related test Climate dependent requirements and related test Precision and dispute methods............., methods................. Annex A (normative) Details of interJaboratory test 2 programme......... ...............7 ...............9 ............. 10 ......................... TURK STAND.AROLARININ TILiF HAKKI TSE'YE AiTiiR. STANDARDIN BU NUSIAS]N]N KULLANItt,I iZNiTSE TARAFINDAN TURKiYE VAGON SANAYiiA_S_'A VER LMiSTiR. BASTLMA't ARiHi: 15.07.2015 TSE'DEN iziN ALTNMADAN STANDARDTN BiR BoLiM0/rAtvAMl ilfiBAs EDiLHi,4Ez. QocALTiLAMAZ. 11 TS EN 590 :2014-02 EN 590:2013 (E) Foreword This document (EN 590:2013) has been prepared by Technical Committee CEN/TC l9 "Gaseous and liquid fuels, lubricants and related products of petroleum, synthetic and biological origin", the secretariat of which is held by NEN. This European Standard shall be given the status of a national standard, either by publication of an identical text or by endorsement, at the latest by March 2014, and conflicting national standards shall be withdrawn at the latest by March 20'14. Attention is drawn to the possibility that some of the elements of this document may be the subject of patent rights. CEN land/or CENELEC] shall not be held responsible for identifying any or all such patent rights. This document supersedes EN 590:2009+A1 :2010. This document has been prepared under a mandate given to CEN by the European Commission and the European Free Trade Association [5] The requirements of the European Fuels Directive 98n1lEC [1], including amendments 2003117|EC 121, 2009/30/EC [3] and 2011/63/EC [4], have been included. Dates are included with all normative test method references in order to comply with the requirements of the European Commission; with the accompanying assurance by CEN/TC 19 that any referenced updated versions will always give samilar accuracy and the same or better precision (see [4]). Significant technical changes between this European Standard and the previous edition are: - lnclusion of the revised EN '14214 FAME specification. - Specific requirements concerning the limitation of use of methylcyclopentadienyl manganese tricarbonyl (MMT) as required by the EC have been incorporated. - Addition of the Fuel lgnition Tester (EN 16144) as an alternate test method to the CFR engine test. - Addition of Simulated Distillation by gas chromatography (GC), EN ISO 3924, as an alternate test method to distillation by EN ISO 3405. - lntroduction of the improved EDXRF determination technique for low sulfur contents, EN ISO 13032, in replacement of EN ISO 20847. Annex A is normative and contains the precision data generated on the test methods, which are the result of inter-laboratory testing, carried out by working groups of CEN/TC 19. Many of the test methods included in this standard were the subject of inter-laboratory testing to determine the applicability of the method and its precision in relation to blends of automotive diesel fuel containing 10 Yo (VN) or higher of different sources of fatty acid methyl esters (FAME). According to the CEN-CENELEC lnternal Regulations, the national standards organisations of the following countries are bound to implement this European Standard: Austria, Belgium, Bulgaria, Croatia, Cyprus, Czech Republic, Denmark, Estonia, Finland, Former Yugoslav Republic of Macedonia, France, Germany, Greece, Hungary, lceland, lreland, ltaly, Latvia, Lithuania, Luxembourg, Malta, Netheriands, Norway, Poland, Portugal, Romania, Slovakia, Slovenia, Spain, Sweden, Switzerland, Turkey and the United Kingdom. TORK SIANDARDLARIN]N TELIF HAKKI TSE.YE AITTiR STANDARDIN BU NUSHASININ KULLAN M iZNI TSE TARAFINDAN TURKiYE VAGON SANAYIi A,S.'A VERILIViSTiR. BASiL[,4A TARiHi: 15.07.20]5 TSE'DEN iZiN ALINMAOAN STANDARDIN B1R AO!UMU,'TAMAIVI iLTiBAS EDiLEI\T1EZ, QOGAITILAIVAZ TS EN 590 : 2014-02 EN 590:2013 (E) 1 Scope This European Standard specifies requirements and test methods for marketed and delivered automotive diesel fuel. lt is applicable to automotive diesel fuel for use in diesel engine vehicles designed to run on automotive diesel fuel containing up to 7 ,0 o/o(Vt\tl Fatty Acid Methyl Ester. NOTE For the purposes of this European Standard, the letms respectively the mass fraction and the volume fraction. 2 "o/o ltn/ml" and ""k (VM" are used to represent Normative references The following documents, in whole or in part, are normatively referenced in this document and are indispensable for its application. For dated references, only the edition cited applies. For undated references, the latest edition of the referenced document (including any amendments) applies. EN 116:'19971), Diesel and domestic heating fuels prEN 12662:2012'?), Liquid petroleum products diesel fuels and tatty acid methyl esters - - Determination Determination of cold fitter plugging point of total contamination in middle distiltates, - EN 12916:20061), Petroleum products Determination of aromatic hydrocarbon types in middle d,Sr//afes High perfomance liquid chromatography method with refractive index detection EN14078:20091), Liquid petroleum products - Determination middle disti ates - lnfrared spectrometry method of fatty acid methyl ester (FAME) content in EN 14214'.20123), Liquid petroteum products - Fatty acid methyl esters (FAME) for use heating applications - Requirements and test methods in dieset engines and EN 15'195:20071), Liquid petroteum products - Determination of ignition delay and derived cetane number (DCN) of middle distillate fuels by combustion in a constant volume chamber EN 15751:20091), Aulomotive fuels - FaW acid methyt ester (FAME) Determination of oxidation stability by accelerated oxidation method fuel and blends with diesel fuel - (DCN) of middle distillate fuels - Fixed range injection period, constant volume combustion chamber method EN 16329:2013, Diesel and domestic heating fuels - Determination of cold filter ptugging point - Linear cooling bath method prEN 16576:2013'?) , Automotive fuets - Detemination of manganese and iron content in middle distillate fuels lnductively coupled plasma optical emission spectrometry (Cp OES) method EN 2301 5:1994, Petroleum products - Determination of ctoud point (lSO 3O1S:1992) EN ISO 2160:1998, Petroleum products - Corrosiyeness to copper - Copper strip test (lSO 2160:1998) EN ISO 2719:2002 , Determination of flash point - pensky-Madens closed cup method (lSO 2719:2002) 1) Under revision. 2) ln preparation. 3) This document is currently impacted by EN 14214:2O12lFptA1:2013. 4 ,oaK sTANDARDLART:'rIN TEL,F HAKK, rsE'yE AirriR. STANDARDTN BU NUSHASTNTN KULLANTM izNi TURKJYE VAGON SANAY|i A,S.'AVERiLMiSTiN BASII MATARiHi ]507,2015 TsE'DEN iziN ALTNMADAN srANDArtoiN BiR u0t [iMti/] AUAMt iL riBAS EDTLETJEZ. CoGALTiLAMAZ rsE TARAFTN,AN TS EN 590 : 2014-02 EN 590:2013 (E) ENlSO3104:1996, Petroleum products - Transparent and opaque liquids viscosiy and calculation of dynamic viscosity (tSO 3104:1994) - Determination of kinematic EN ISO 3'170:2004, Petroleum liquids - Manuat sampling (lSO 31tO:2004) EN ISO 317'l:19991), Petroleum tiquids - Automatic pipeline sampling (tSO 31t1:1988) EN fSO 3405:2011 , Petroleum products - Determination ot distiltation characteistics at atmospheric pressure (lSO 3405:2011) EN ISO 3675:1998, Crude petroleum and liquid petroleum products Hydrometer method (lSO 3675:1998) EN ISO 3924:2010, Petroleum products method (lSO 3924:2010) - Laboratory determination of density - - Determination of boiling range distibution EN|SO4259:2006, Petroleum products - methods of test (lSO 4259:2006) EN ISO 4264:20074), Petroleum products - Gas chromatography Determination and apptication of precision data in relation to - Calculation of cetane index vaiable equation (lSO 4264:2007) EN ISO 5165:19981), Petroleum products - Determination of the ignition method (lSO 5165:1998) of middle-distillate fuels qual| of dieseltuets - by the four- Cetane engine EN ISO 6245:2002 , Petroleum producls - Determination ofash f/SO 6245:2001) EN ISO 10370:1995, Petroleum products - Determination of carbon residue - Micro method (tSO 10370:1993) EN ISO 12156-1:2006, Diesel fuel - Assessment of /ubrlc ity using the high-frequency reciprocating rig (HFRR) - Pad 1:Test method (lSO 12156-1:2006) EN ISO 12185:1996, Crude petroleum and petroleum products - Determination method (lSO 1 21 85: 1 996) EN lSO 12205:1996, Petroleum products (tSO 12205:1995) - Determination of density - Oscitlating U-tube of the oxidation stabitity of middle-distitlate EN ISO 12937:200Q, Petroleum products - Determination of water - Coulometric (tSO 12937:2000) Kal fuets Fischer titration method EN ISO 13032:2012, Petroleum products - Determination of low concentration of suffur in automotive fuels Energy-dispersive X-ray fluorescence spectrometic method (lSO 1 3032:ZO1 2) EN ISO 13759:1996, Petroleum products - Determination of alkyl nitrate in diesel fuels (lSO 13759:1996) EN ISO 20846:20'1 1, Petroleum products fluorescence method (lSO 20846:201 1 ) - - Spectromatric method Determination of sulfur content of automotive fuels EN ISO 20884:201 1, Petroleum products - Determination of sulfur content of aulomotive fuets dispersive X-ray fluorescence spectrometry (l SO 20A84:201 ) - - lJttraviolet Wavelength- 1 4) This document is currently impacted by EN tSO 42U:2007 tA1.2013. lURK SfANDARDLARININTELiF HAK(1]SE'YE AiTTiR STANDARoIN BU NOSHASIN1N KULLANIM izNiTSE TARAFIN TORKiYE VAGON SANAYI VERIiMiSTiF I ASILMA TABiHi' 15 07 2015 TSE'DEN lZiN ALINi/ADAN ^1.S.'A S] ANDARDIN BiR B( LUMU,TAMAVI,LTiaAS ED'LEMEZ. CCGALTITAMAz 5 TS EN 590 :2014-02 EN 590:2013 (E) 3 Sampling samples shall be taken as described in EN lSo 3170 0r EN tso 3171 and/or in accordance with the requirements of national standards or regulations for the sampling of automotive diesel fuel. The national requirements shall be set out in detail or shall be referred to by reference in a NationalAnnex to this European Standard. ln view of the sensitivity of some of the test methods referred to in this European Slandard, partacular attention shall be paid to compliance with any guidance on sampling containers which is included in the test method standard. 4 Pump marking lnformation to be marked on dispensing pumps used for delivering automotive diesel fuel, and the dimensions of the mark shall be in accordance with the requirements of natio-nal standards or regulations for the marking of pumps for automotave diesel fuel. Such requirements shall be set out in detail oi shall be referred to by reference in a National Annex to this European Standard. Labelling shall be clearly visible, easily legible and displayed at any point where diesel with metallic additives is made available to consumers. The label shall coniain: "Contains metallic additives' in the language(s) and shall be laid down in the NationalAnnex to this document. 5 national Requirements and test methods 5.1 Dyes and markers The use of dyes or markers js allowed. 5.2 Additives 5.2.1 General ln order to improve the performance quality, the use of additives is allowed. Suitable fuel additives without known harmful side-effects are recommended in the appropriate amount, to help to avoid deterioration of driveability and emissions control durability. other technical means with equivalent effect may also be used. loTF developed. Deposit forming tendency test methods suitable for routine control purposes have not yet been identified and 5.2.2 Methylcyclopentadienyl manganese tricarbonyl (MMT) When methylcyclopentadienyl manganese tricarbonyl (MMT) is used, a specific labelling is required (see also Clause 4). MMT is a metallic additive that can be used in diesel. The presence of the MMT in diesel shall be timited of manganese per ritre from 'r January 2011. The rimit shal be 2 mg of manganes" p"i ritr" to tro, 1 January 2014. 6 mg NoTE These requirements are subiect to review following an assessment by the European commission. 5.3 Fafty acid methyt ester (FAME) Diesel fuel may contain up to 7,0 % (vM ol FAME complying with EN .14214:2012, in which case the ctimatedependent requiremenls set out in S.4.2 of EN 14214.201i dL not appty. NOTE 1 A suitabre method for the separation and identification of FAME is given in EN 14331 [6]. TIJRK STAND.ANDIAF}NIN TEL hAKXI TSE'YE A TTiN. STANSARDIN AU NUSHAS1NIN Kt]LLAN1]\4 iZNi TSE TARAFINDAN IURKiYf VAGON SANAYiT A S ,A VER LMiSTiH. Elrls Ua I nn+lt, t5.02 20t5 aSE DEN rzrN ALTNMADAN SIANDAaDtN aiR BOLuv,l, rqr,,rov, ,r t,aeS gOCar lJ,L rr,rez. r rt eluZ. TS EN 590 :20i4-02 EN 590:2013 (E) climate dependent requirements flyE as a blending component for use in diesel fuel according to this document are set out in 5 4.3 of P.l EN 14214:2012. rn" ri""itic grao"s shall be specified on a national basis according to locat climatic conditrons and the FAME volume in ihe diesel fuel. The finished blend of diesel fuel shall also comply with the climate dependent requirements set out in 5.6. of this document. cold flow additives, when used in FAME, should be specificafiy matched to the base diesel fuel and FAME quality to ensure conect performance.consistent with the requirJments set out in this European standard. The choice could result in incompatibility between tne coto ttow'aoJitives used in the FAME and the diesel fuel. The choice of cold flow additive technology should be a matter between the fuel blender and the FAME supplier taking into account the cli;;tic-dependent "ontr"ctr"l reffiments or the finished dieset fuel. 2 cold ffow requirements for FAME as a blend component in diesel fuel are set out an Tables 3a and 3b and the National Annex of EN 14214:2012. in order to or satrratea monogtycerides in the final EN 590 blend to ensure trouble-free operation. work is "ontror on-going to ioentirv"onient a iurtaore test method for saturated monogtyc€rides or l a performance test to control this aspect of tow temierjure NorE - ,"rirl, p",f;,f;;e ln order to improve the oxidation.,stability of FAME, it is strongly recommended to add oxidation stabitity . enhancing additives to FAME at-the production stage and'beiore storage, providing an oxadation stability similar to that obtained with 1 ooo,mgikg.or z o-ol-te-rt-uutylJ--hydroxytolrene (BHT, officially designated by IUPAC as 2,6-bis(.1, 1 -dimethytethyt)-4_mJtnytphenog. The- similar action may be read as providing oxidation stability performance at least equal to that obtained with 1 000 mg/kg of BHT. cAUTloN There is a potential risk of precipitate formation with oxidation stability enhancing - low additives at temperatures in low aromatic i."iic trei.'6"rtion shoutd therefore be taken in the choice of oxidation stability enhancing aoOltives to aiciic ar"O" feUe. 5.4 Other (bio-) components Limits for addlng FAME are set for technical reasons. Limits for IAME d9 not apply to other (renewabte) hydrocarbons such as Hvdrokeated veg_etabre oir cas io Liquid (GTL) or'ei6,n"., io iiqrio (erl) tHvoi derived hydrocarbons' since these paraffinic oieser coffinenis are aflowed in any proportions provided that the final blend complies with the requirements of eN sgo. in" ,." ot r"n.*rble feedstock at refineries is also allowed provided that the final fuel meets the requirem"nt. oief.iSSO. NOTE A draft fuel specification for paraffinic diesel fuel has been developed [7]. 5.5 Generaily appricabre requirements and rerated test methods 5'5'1 when tested by the methods indicated In Table 1, automotive diesel fuel shall be in accordance with the limits specified in Tabre 'r. The test methods risted in Tabie t have been assessed for apprication to automotive dieser containing FAME. precision data from inter-raooratory test programmes are given in normative Annex A, where these were found to be different froni tne precision data given in the test methods for neat petroleum products. 5'5'2 The limiting value for the carbon residue given in Table '1 is based on product prior to addition of ignition improver, if used. lf a value exceeding the limit'is out.in"Jo-n nn-i.t'"d fuel in the market, EN lso 13759 shall be used as an indicator of the presence of a nitrate-containingcompound. lf an ignition improver is thus proved present, the rimit varue for the carbon r"rior" oitt pioo"rct under test cannot be appried. additives does not exempl the manufacturer tro, " ih"-requirement of maximum 0,30 o/oThe use of ,*"iing" rm/m) or carbon residue prior to addition of additives 5'5 3 Diesel fuel shall be free from any adulterant or contaminant that may render the fuel unacceplable for use in diesel engine vehicles. NorE For further information on preventrng contamrnation by water or sedfient that may occur in the suppty charn or for cross-contaminarion. it is advisabre ro ciiirnn i r s367_3 lgj respectivery. "r,,"& iioiliiii ".'cerna TI]RKS'ANL,^P',OR\,\-IIII*A"I-'I,YL,AT'IR5.A\NAOIII\6U\L\IIASININKIJLLAN,MZNISF-ANA|INDA\ IIIRK!r r^GoN\AN4,,.^S /ivt t..Mrst,) h.\stt vA,A*,r,, .5r1l,0tr '..-. rsE'DEN iziN ALINMADAT! sreNoenorN arn a(jLo-^,itj,i,rri,iii"r]iria-["]LEMEz. cocALrLA[.{Az. 7 TS EN 590 : 2014-02 EN 590:2013 (E) Table 1 - Generally applicable requirem6nts and test methods for automotive diesel fuel Property Unit Cetane number Limits mtntmum maximum 51,0 Test method " (See Clause 2) D EN ISO 5165 EN 15195 Cetane index EN 16144 EN rSO 4264 46,0 Density at 15 "C kg/m3 Polycyclic aromatic hydrocarbons Sulfur content d 820,0 845,0 % (m/ml 8,0 mg/kg Manganese content r until 2013- 12-31 from 2014 to 01-Ol onwards '10,0 mg/l EN tSO 3675 c EN tSO 12185 EN 12916 EN rSO 20846 " EN tSO 20884 EN ISO 13032 prEN 16576 6,0 2,0 Flash point Above 55,0 s EN tSO 2719 Carbon residue (on 10 % distillation residue) Ash content o/o Water content m9/kg 200 EN Total contamination mg/kg 24 EN 12662 Copper strip corrosion (3 h at 50 :C) rating Fatty acid methyl ester (FAME) contenti %(vM oxidation stabitty % (m/m) l 0,30 (m/m) 0,010 class Lubricity, corrected wear scar diameter (wsd 1,4) at 60 "c Viscosity at 40 "C 7,0 pm mm'/s (VM rccovercd at 250 'C Yo (VM recovercd at 350 'C 95 % (UM recovered at o/o Yo o/o (VM (VM 'c rso 12937 h rso 2160 EN '14078 EN tSO 12205 20 Distillation r'l EN tSO 6245 EN 1 g/m' h EN tSO 10370 EN 15751 460 2,000 EN lso'12156-1 rso 3104 4,500 EN <65 EN tSO 3405 EN rSO 3924 ' 85 360 NoTERequirement5inboldrefertotheEuropeanFuetsolre 2009/30/EC I3l and 2011/63/EU [4]. See also 5.7.4. See also 5.7.2. For the purposes of this European Standard, polycyclic aromatic hydrocarbons are defined as the total aromatic hydrocarbon contenl less the mono-aromalic hydrocarbon content, both as detemined bt EN 12916. See also 5.7.3. See also 5.2.2. See also 5.5.2 and Annex A. Further investigation into the total contaminalion test method to improve the prec.ision, particularly in lhe presence of FA[4E, is being canied out by CEN. FAME shall moet tho roquirements of EN 14214, soe [31. j When dieselfuel contains more than 2 %(V/v) FAME, oxidation stability as determined by EN .ls7sl is lhe requirement. For the calculation of the cetane index the 10 o/o, 50 % and 90 o/o recovery poinls are also needed. ry 4 I The limits for distirration at 250 "c and 350 'c are induded fordieserfuer in rine with EU common customs tariff. EN ISO 3924 gives instrudions to convert to ISO 3405€quivalent data. See also 5_7.5. 8 TURK STANDARDLARININ 'I E LiI iTAKKITS:'YE AITTIR STANDARD N BU NUSHASININ KULLANIM iZN] TURKiYE VAGON SANAYiTA.S. A VERiLMiSTaR. aAStL[,4A TARiFi] t5 07 2Oi5 TSE'DEN iZiN ALINMADAN STANOARDiN BiR AOLUMU/TAMAMI ]LTiBAS EDiLEMEZ. COGALTILAMAZ- ]SE TARAFINDAN TS EN 590 :2014-02 EN 590:2013 (E) 5.6 Climate dependent requirements and related test methods 5.6.1 For climate-dependent requirements, options are given to allow for seasonal grades to be set nationally. The options are for temperate climates six CFPP (cold filter ptugging point) gradei and for arctic or severe winter climates five different classes. Climate-dependent requirements ire given in Table 2 (temperate climates) and Table 3 (arctic or severe winter climates). When tested by the methods given in Table 2 and Table 3, automotive diesel fuel shall be in accordance with the limits specified in these tables. Table 2 Property - Climate-related requirements and test methods Unit Temperate climates Limits Grade "C, max. CFPP - A Grade B +5 0 Test method Grade Grade c -5 Grade Grade D E F -10 -15 -20 ' (See Clause 2) EN 116 EN 16329 See also 5 Table 3 7.1 - climate-related requirements and test methods Pro perty Units CFPP "C, max. Cloud point "C, max. Density at 15 "C kg/m",min. Viscosity at 40 'C Cetane number EU e - Arctic or severe winter climates class class Limits class class class 0 1 2 3 4 -20 -26 -32 -38 -44 EN'116b -34 EN '16329 EN 23015 Test method -10 -'16 -22 800,0 845,0 800,0 800,0 kg/m3, max. 800,0 845,0 840,0 840,0 800,0 840,0 mm2/s, min. mm2/s, max. 1,500 1,500 1,500 4,000 4,000 4.000 1,400 4,000 't ,200 4.000 51 ,0 51,0 51 .0 51 ,0 m tntmum 51 .0 a (See Clause 2) EN rSO 3675 " EN ISO 12185 EN lso 3104 EN tso 5165 d EN 1 5195 EN 16144 Cetane number r Cetane index Distillation e mtnrmum 49,0 49,0 48,0 47 ,0 47 ,0 minimum 46,0 46,0 46,0 43,0 43,0 h recovered at 180 "C o/o recovered at 340 "C o/o (VlV), max. 1 0,0 10,0 1 0,0 10,0 1 (VM, min. 95,0 95,0 95,0 95,0 95,0 0,0 EN EN EN EN tSO 5165 15195 16144 ISO 4264 EN tSO 3405 EN rSO 3924 d I See also 5.7.1. See also 5.7.6. See also 5.7.2. See also 5.7.4. Il^:9^T!1i9..-.*h"le the !]l-9o_ujEigg--where the European Fuels Directive 98/70 EC[1] inctuding amendments 2@3nZEC European Fuels Direclive 98/70 EC[1] incruding amendments 2oo3tiltEC 2009/30/EC [3] and 20'11/63/EU [4] appties. l2), I2l, 2@9/30/EC [3] and 2011/63/EU [4] does not appty. EU Common Customs Tariff definition of gas oil may not apply to the grades defined for use in arctic or severe winter climates For the calculation of the cetane index the uee atso 5. /.5 io ok (vM, 50 % (vM and go o/o (y/y) recovery points are also needed. T,RK-STANDAROLARININ TELiF HAKKI TSE'YE AiTTIR, STANDARDIN BU NUSHASININ KULLANIM iZNiTSE TARAFINDAN TURKryE VAGON SANAYIi A.S_ A VERiLMiSliB. AASttMA IARaHir t 5 07.2015 TSE'DEN iZiN ALINMADAN STANDARDIN BiR AOLLJMU/tAMAMI iLTiBAS EDiLEMEZ, COGALTILAMAZ 9 TS EN 590 : 2014-02 EN 590:2013 (E) 5'6'2 ln a National Annex to this European Standard, each country shall detail requirements for a summer and a winter grade and may include (an) intermediate and/or regional grade(s) which shati be lustitieo by national meteorological data. 5.7 Precision and dispute 5'7'1 AII test methods referred to in this European Standard inctude a precisaon statement. ln cases of dispute' the procedures for resolving the dispute and interpretation of the results based on tesr method precision, described in EN ISO 4259. shall be used 5.7.2 ln cases of dispute concerning density, EN ISO 3675 5.7.3 ln cases of dispute concerning sulfur content, either EN sha be used. lso 20846 or EN lso 20884 shalt be used. 5'7.4 ln cases of dispute concerning cetane number, EN ISO 5165 shall be used. For the determination of cetane number alternative methods to those indicated an Table 1 and Table 3 may also be used,-piovided tnat these methods originate from a recognised method series, and have a valid precision statement, derived in accordance with EN lSo 4259, which demonstrates precision at least equal to that of the referenced method. The test result, when using an alternative method, shall also have a demonstrable relationstrip io tire resutt obtained when using the referenced method. 5.7.5 ln cases of dispute concerning distillation, EN ISO 34OS 5.7.6 ln cases of dispute concerning CFpp, EN 10 1 sha be used. 16 shall be used TUBI( STANDAADLARININ TELIF I]AKhI TSE YE.AiTTiR SIANDAROIN _' iZNi TSE TARAFINDAN TURhr/tVACO^JSANAYIASAVt q"M,St.n BASrt Vp tAor-r..f BU NOSHASININ KULLANIM TSE'DEN iziN ALtNMAI)AN SIaNDARDIN BrF BoLitr,,lunalllaur O,ZittS " irria"aiiollaMEz. CocALTlrAMAz. TS EN 590 : 2014-02 EN 590:2013 (E) Annex A (normative) Details of inter-laboratory test programme T€bleA:1 presents the precision data obtained in inter-laboratory testing programmes by CEN/TC 19 [10] and the El [11], that differ from those of test methods listed in Tabli t anO that at the time of pubtication of this European Standard were not yet revised. NOTE values: Ash The following methods were found to have precision data for 5 % (vM F AME btends simitar to the pubtished content. EN ISO 6245, Oxldation stability: EN tSO 12205, CFPP: EN 116. Table A.1 Property - Precision data updates Test method Unit 5 Viscosity at 40 "C EN rSO 3104 mm'/s CEN/TC 19 data for Yo (VM FAME blend r= 0,001 1X R=0,018X r=2,0 Flash point EN tSO 2719 Carbon residue EN tSO '10370 R=3,5 r=0,1430.f5 R=0,2125.Xos Mrere r R X is repeatability (EN tSO 4259) is reproducibitity (EN tSO 4259) is the mean of two results being compared TORK STANDAROLARININ TE!'F HAKKI TSE'YE AiTTiR- STANDARDIN BU NOSHASININ KULLAN}M iZNiTSE TARAFINDAN IURKYE VAGON SANAyiiA_S..A VERiLt\,iiSTiR. BASILMA rARiHi: 15.07201t TSE'DEN iziN ALINMADAN STANDARDIN BiR aoLtuuteruarvr rrrdei-iolLEMEz. QocALTTLAMAZ_ 11 TS EN 590 :2014-02 EN 590:2013 (E) Bibliography t1l Directive.gErolEc of the European parriament and of the councir of 13 october .r99g rerating to the quality of petrol and diesel fuels and amending Council Directive g3tlZlEEC 12) Directive 2003/'17lEc of the European parriament and of the councir of 3 March 2oo3 amending Directive 98/70/Ec relating to the quality of petrol and djeset fuels and amending Councit oirective 93t12tEEC I3l oirective 2009/30/EC of the European parriament and of the councir of 23 Aprir 2009 amending Directive 98/70/Ec as regards the specification of petror, oieseiano gas-oir and introducing a " mechanism to monitor and reduce greenhouse gas emissions and amending councir Directive '1999/32lEC as regards the specification of fuer ised by inrand walerway vessers and repearing Directive 93/12lEEC 14) Directive 201 1/63/EU of 1 June 2011 amending, for th€ purpose of its adaptation to technicar progress, Directive 98/70/EC of the European parriamenland ot tne iouncrt retating to the quarity or peiroi'"J diesel fuels tsI Mandate M/394 - Mandate to cEN on the revision of EN sgo to increase rhe concentration of FAME and FAEE to 10o/o vlv, 13 November 2006 t6l EN 14331:2004, Liquid petroleum products - Separation and characterisation esters (FAME) from middre disti ates - Liquid chromatography (Lc)/gas t7) cEN/TS 15940, Automotive fuers - paraffinic ctiesel fuel from synthesis or hydrotreatment Requirements and tes, methods t8l CEN/TR 15367-1 , Petroreum products - Guide for good housekeeping - pad tel CEN/TR 15367-3, petroreum products - Guide tor good housekeeping - paft [10] of fatty acid methyl chromatogiapny Gc1';etnoa 12 . Automotive dieset fuers 3. cross contamination cEN/TR 15'160, Petroreum and rerate.d products - Appricabirity of dieset fuet test methods for Fatty Acid Methyl Esters (FAME) - tnformation and resutts on ,ounO [11] 1 ioii tests El Research Report on lp 398 and EN ISO 10370, under publication, - avaitable from the Energy lnstitute, 6 1 New Cavendish Street, London WI G ?AR, engfanJ rELiF rrAKKr rsE'yE ArrriR. STATDARDTN *?I5ililDjlplllllliN TURKVE vAGoN sANAy iA s.,A vERtMisriR. aAsrL n,te BU NU.HASTNTN KULLANTM ririr.,-rr,,.iIor zors izN,rsE TARAF,NDAN TSE,DEN iziN ALINMADAN STANDARDjN ain aoL iLIaij,ieLl;.MI.;I i Ii;As ToiLEMFZ. coGALTILAIJAZ